Electron-Stimulated
Ion Desorption
The
Electron-Stimulated Ion Desorption (ESID) effect in
Bayard-Alpert gauges is caused by ionization of adsorbed
gas molecules on the electron collector by the arriving
electrons. These ions then are driven by the internal
electric fields in the gauge to the collector, along with
the ions formed from the gas phase. The result is a
falsely high apparent pressure measurement which gets
proportionally worse as the pressure falls. ESID errors
exhibit themselves as false high pressures or
prolonged/inconsistent pump-down times and are noticeable
at pressures as high as 10-7
Torr.
General
Vacuum Practice
To
insure that the measured pressure accurately mirrors the
system pressure, several factors should be considered.
The gauge should be well de-gassed, especially when
measuring very low pressures. The gauge should be baked
under high vacuum for one hour at a temperature of at
least 250
C
or as high as is practical up to the maximum set by the
particular gauge specification. The internal electrodes
are de-gassed by heating them to a temperature of about
900
C
for approximately 15 minutes. The electrode heating is
accomplished by either electron bombardment (EB) or by
passing a high current at low voltage (I
R)
through the grid. Gauges equipped with squirrel-cage
grids or those where the grid wire is welded, brazed or
swaged to the support wire at multiple locations are
usually only de-gassed by electron bombardment. The
collector in present designs can only be de-gassed by
electron bombardment. Grids consisting of a helix or
double helix with both ends having external connections
can be de-gassed by either the EB or high current
I
R
method. Care must be taken to have a heavily grounded
gauge circuit and to avoid touching exposed electrodes
especially during EB de-gas when higher voltages are
present.
The
ionization gauge has a certain pumping capacity due to
both chemical and electrical effects. Chemical pumping is
due, in general, to reactions on the hot filament and the
adsorption of gases on very clean surfaces. As the
surface becomes saturated the pumping decreases. Pumping
due to electronic phenomena continue as long as voltages
are applied.
The
vacuum connection between the ionization gauge and the
rest of the system can have a great effect on the
measuring ability and life of the gauge. If the
tubulation has too small a diameter or is connected by
long plumbing to the vacuum system, the gauge reading may
differ from the system pressure by as much as a factor of
ten. This difference is most pronounced when system
pressures change rapidly and the system is at low
pressures. It is wise to select the largest diameter
tubulation possible or even use a nude gauge in the
vacuum system. A glass gauge with 3/4-inch tubulation has
adequate conductance for use down to the
10-8
Torr scale. A gauge with 1-inch tubulation can be used
down to the 10-10
Torr.
When
considering gauge placement and tubulation size, a number
of factors can come into play. If the application is one
where material is evaporated or sputtered, care must be
taken to keep the material out of the gauge.
Contamination of the gauge can severely limit life and
lead to grossly inaccurate measurements. Also, operations
taking place in the 10-2
to 10-4
Torr
range, with relatively high voltage and current, can lead
to long path arc discharge. A simple right-angle
connector has been shown to lessen both the long path arc
and evaporation problems, but with some sacrifice of
conductance.
Manufacturer's
Cross Reference
Each
manufacturer's gauge is made to custom requirements and,
therefore, generic gauges purchased from unknown "second
sources" should be approached with caution. In some
cases, generic material or approximate tolerances are
used. These generic gauges may not perform as intended by
the original manufacturer or are of inferior quality. It
is, therefore, recommended that you contact the original
manufacturer of the gauge to assure that complete
operational specifications are met. In the cases where
the original manufacturer no longer provides this gauge,
they can best guide you to a reliable source of gauges.
Several companies, no longer in operation, have made
arrangements with ETI to provide gauges that meet the
exact original specifications. If you are uncertain about
the source of your replacement gauges, please contact
ETI.